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Purity:99%
Stable crystalline forms of a compound r...
Boc-Aib-OH
N-hydroxybenzenecarboximidamide
C11H13N3O*ClH
| Conditions | Yield |
|---|---|
|
Boc-Aib-OH;
With
N-ethyl-N,N-diisopropylamine; isobutyl chloroformate;
In
1-Propyl acetate;
at 0 ℃;
for 1h;
N-hydroxybenzenecarboximidamide;
In
1-Propyl acetate;
at 0 - 95 ℃;
for 6h;
With
hydrogenchloride;
In
water;
for 2.5h;
|
92.7% |
C11H13N3O*ClH
methyl chloroformate
C12H11N3O2
| Conditions | Yield |
|---|---|
|
C11H13N3O*ClH; methyl chloroformate;
In
water; toluene;
at 50 ℃;
for 1h;
Alkaline conditions;
With
boron trichloride; triethylamine;
In
toluene;
at 50 ℃;
for 2h;
|
Boc-Aib-OH
N-hydroxybenzenecarboximidamide
C34H36N4O7
17-(cyclopropylmethyl)-6,7-didehydro-4,5H-epoxy-3,6,14-trihydroxy-N-[2-(3-phenyl-1,2,4-oxadiazol-5-yl)propan-2-yl]morphinan-7-carboxamide 4-methylbenzenesulfonic acid tosylate
Naldemedine
C12H11N3O2
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